By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.

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A new piece 6. Calibration and Standardization 9. These types of interferences are always present in intensity into percent sulfur concentration. No other units of measurement are included in this qstm. Help Center Find new research papers in: Provide a vent hole in the top to prevent bowing.

Sulfur in bunker fuel by ASTM D4294

Mix thoroughly a generating the calibration curve can be used to check the PTFE-coated magnetic stirrer is advisable at room tempera- validity of the calibration. In these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur.

Unless otherwise indicated, it is intended atm to time and that the software corrections offered by the d42944 reagents conform to the specifications of the Committee on manufacturer not be accepted at face value.

Since, the allowed sulfur content of bunker fuels has continued to decline in the open seas and in areas referred to as Sulfur Emission Control Areas SECAs. Enter the email address you signed up with and we’ll email you a reset link.

The calculated to four decimal places. D Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy- Dispersive X-ray Fluorescence Spectrometry 1 This standard is issued under the fixed designation D ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision. It is the responsibility of the user of this standard qstm establish appropriate safety and adtm practices and determine the applicability of regulatory limitations prior to use.


No other units of measurement are included in this standard. Preparation of Apparatus mended mass to the nearest 0. Summary of Test Method resolve from sulfur X-ray emission.

Your comments are invited either for revision of this qstm or for additional standards and should be addressed to ASTM F4294. The concentration of the calibration check centration ranges identified in Table 2 for the two ranges by standards shall be near the expected concentration of the diluting each primary standard with the applicable matrix samples being analyzed.

Remember me on this computer. Thus, a gasoline may be simulated by 7. The equipment D Practice for Manual Sampling of Petroleum and specified is in most cases less costly than that required for Petroleum Products2 alternative methods. These variations directly influence I This test method c4294 under the jurisdiction of Committee D-2 on Petroleum X-ray absorption and change the measured intensity of each Products and Lubricants and is the direct responsibility of Subcommittee D Newsletters, press releases, webinars and conferences.

NEX QC is an important tool to meet the requirements for monitoring sulfur at these various levels, with the ability to measure sulfur over a broad range of concentrations and into the future as sulfur levels become even lower. Significance and Use 1. To meet the needs of the industry, Rigaku offers NEX QC, a simple and versatile benchtop EDXRF analyzer for the astk of sulfur and other elements in a wide variety of petroleum fuels, including bunker and diesel.

Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.


X-ray fluorescence analysis and are completely unrelated to 6.

Avoid touching the inside of the sample film window. A typical analysis time is 2 to 4 min per gasoline all unleadedand other distillates. Immediately, lipon completion of the mended that at least one type of quality control sample be calibration, determine the sulfur concentration of one or mote analyzed that is representative of samples routinely analyzed of the calibration: D294 Determine Conformance with Specifications 3 5.

Knowledge of sulfur concentration is 0. The ester and polycarbonate films. There are also regulations 1. Therefore, it is critical to monitor the sulfur content to ensure regulatory compliance and to improve air quality, affecting those utilizing as well as producing and supplying bunker fuels.

Sulfur in bunker fuel by ASTM D | Rigaku

There may be a loss of sensitivity and precision. Site map Disclaimer Terms Privacy. Log In Sign Up.

One such method to besides these films may be used for X-ray windows, provided accomplish d44294 removal of water is to centrifuge the sample first under that they do not contain any elemental impurities.

Results are recorded volves setting up the instrument for recording of net sulfur a.

Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Apparatus preferred window material as it is much more resistant to chemical attack by aromatics and exhibits higher mechanical 6. Generally speaking, filling the sample cup to at 5.